N-[3-Phenyl-1-(2,3,5,6-tetrachloro-4-hydroxyphenoxy)prop-2-enylidene]aniline
✍ Scribed by Hu, Xiu-Rong ;Gu, Jian-Ming
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 241 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.040 wR factor = 0.117 Data-to-parameter ratio = 13.9
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
The title compound, C 13 H 14 ClN 5 O, was synthesized from 2,4dichloro-6-morpholino-1,3,5-triazine and aniline. In the crystal structure, there are intermolecular N-HÁ Á ÁO hydrogen bonds which propagate infinite chains parallel to the c axis. The morpholine ring adopts a chair conformation.
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.005 A Ê R factor = 0.035 wR factor = 0.090 Data-to-parameter ratio = 11.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The enone fragment, the thiophene ring and the benzene ring of the title molecule, C 13 H 9 ClOS, are all essentially individually planar. The thiophene ring is disordered over two sites, corresponding to a rotation of approximately 180 about the single C-C bond to which it is attached. The crystal