𝔖 Bobbio Scriptorium
✦   LIBER   ✦

N-(3-Cyano-2-oxo-2,5,6,7,8,9-hexa­hydro-1H-cyclo­hepta­[b]­pyridin-1-yl)-4-methyl­benzene­sulfon­amide

✍ Scribed by Elgemeie, Galal H. ;Mahmoud, Mahmoud A. ;Jones, Peter G.

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
276 KB
Volume
58
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

2-Methoxy-4-methyl-6,7,8,9-tetra­hydro-5
2-Methoxy-4-methyl-6,7,8,9-tetra­hydro-5H-cyclo­hepta­[b]­pyridine
✍ Albov, Dmitry V. ;Rybakov, Victor B. ;Babaev, Eugene V. ;Fedyanin, Ivan V. ;Asla 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 172 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.003 A Ê R factor = 0.067 wR factor = 0.165 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-(4-Chloro­phen­acyl)-4-methyl-6,7,8,9-
1-(4-Chloro­phen­acyl)-4-methyl-6,7,8,9-tetra­hydro-5H-cyclo­hepta­[b]­pyridin-2(1H)-one
✍ Albov, Dmitry V. ;Rybakov, Victor B. ;Babaev, Eugene V. ;Aslanov, Leonid A. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 203 KB

In the pyridone ring of the title compound, C 19 H 20 ClNO 2 , single and double bonds alternate, though allowing some degree of conjugation. One C atom in the cycloheptene ring is disordered over two positions, which form boat and chair conformations of cycloheptene, respectively.

1-(4-Chloro­phen­acyl)-4-methyl-5,6,7,8,
1-(4-Chloro­phen­acyl)-4-methyl-5,6,7,8,9,10-hexa­hydro­cyclo­octa­[b]­pyridin-2(1H)-one
✍ Albov, Dmitry V. ;Rybakov, Victor B. ;Babaev, Eugene V. ;Aslanov, Leonid A. 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 235 KB

In the pyridone ring of the title compound, C 20 H 22 ClNO 2 , single and double bonds alternate, though allowing some degree of delocalization. Two C atoms in the cyclooctene ring are disordered, indicating some ¯exibility of the large ring.