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N-(3-Chloro­phen­yl)-2-{[(1E)-(4-methyl­phen­yl)methyl­ene]amino}-4,5,6,7-tetra­hydro-1-benzothio­phene-3-carboxamide

✍ Scribed by Anilkumar, G. N. ;Kokila, M. K. ;Puttaraja, ;Mohan, S. ;Majunath Shetty, K. S.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
193 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

for data collection on the CCD facility, and organic papers o2842 Anilkumar et al. C 23 H 21 ClN 2 OS

📜 SIMILAR VOLUMES

4,5-Dimethyl-N-(2-methyl­phen­yl)-2-{[(1
4,5-Dimethyl-N-(2-methyl­phen­yl)-2-{[(1E)-(3,4,5-trimethoxy­phen­yl)methyl­ene]amino}thio­phene-3-carboxamide
✍ Vasu, ;Nirmala, K. A. ;Chopra, Deepak ;Mohan, S. ;Saravanan, J. 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 274 KB

The conformation of the title molecule, C 24 H 26 N 2 O 4 S, is influenced by intramolecular N-HÁ Á ÁN hydrogen bonding, andinteractions link the molecules into centrosymmetric dimers. The crystal packing is further stabilized by weak intermolecular C-HÁ Á ÁO hydrogen bonds.

(2E)-1-(4-Chloro­phen­yl)-3-[4-(methyl­s
(2E)-1-(4-Chloro­phen­yl)-3-[4-(methyl­sulfan­yl)phen­yl]prop-2-en-1-one
✍ Harrison, William T. A. ;Yathirajan, H. S. ;Narayana, B. ;Mithun, A. ;Sarojini, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 186 KB

The geometrical parameters for the title compound, C 16 H 13 ClOS, are normal. The dihedral angle between the two benzene rings is 48.16 (5) . The non-centrosymmetric crystal packing is consistent with the substantial non-zero second harmonic generation response.

The 0.893/0.104/0.003 cocrystal of 1-(4-
The 0.893/0.104/0.003 cocrystal of 1-(4-methyl­phen­yl)-3-(3,4,5-trimethoxy­phen­yl)prop-2-en-1-one, 3-(3-chloro-4,5-dimethoxy­phen­yl)-1-(4-methyl­phen­yl)prop-2-en-1-one and 3-(3,5-dichloro-4-methoxy­phen­yl)-1-(4-methyl­phen­yl)prop-2-en-1-one
✍ Ng, Shea-Lin ;Razak, Ibrahim Abdul ;Fun, Hoong-Kun ;Patil, P. S. ;Dharmaprakash, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 387 KB

In the title cocrystal, 0.893C 19 H 20 O 4 Á0.104C 18 H 17 ClO 3 Á-0.003C 17 H 14 Cl 2 O, the crystal packing is stabilized by weak intermolecular C-HÁ Á ÁO and C-HÁ Á Á interactions.