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N-{(1R*,5S*,7R*)-6-Oxobicyclo[3.2.0]hept-2-en-7-yl}phthalimide, C15H11NO3

โœ Scribed by Sheldrick, B. ;Akrigg, D. ;Page, M. I. ;Agathocleous, D.


Book ID
114502294
Publisher
International Union of Crystallography
Year
1984
Tongue
English
Weight
312 KB
Volume
40
Category
Article
ISSN
0108-2701

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Synthesis of (5R,6S)-6-[(1R)-hydroxyethy
โœ J. E. Swigor; C. U. Kim; K. A. Pittman ๐Ÿ“‚ Article ๐Ÿ“… 1988 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 198 KB

The synthesis of the title compound (4) is described. ## Treatment of (3S)-[(lR)-hydroxyethyl]-(4R)- [ 3-(p-nitrobenzyloxy) carbonyl-2-0x0-[ 2-I4C] -3-diazopropan-l-yl]azetidin-2-one1 with rhodium diacetate achieved ring closure forming (5R,6S)-pnitrobenzyl-6-~(1R)-hydroxyethyl]-3,7-dioxo-[3-14C]