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Multiple Quantum 13 C NMR Spectroscopy in Solids under High-Speed Magic-Angle Spinning †

✍ Scribed by Oyler, Nathan A.; Tycko, Robert


Book ID
126201734
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
187 KB
Volume
106
Category
Article
ISSN
0022-3654

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We determine the decay rate constants of zero-, double-and single-quantum coherence for 13 C spin pairs in magic-angle-spinning solid-state NMR. The double-quantum coherence is excited by a C7 pulse sequence and converted into zero-quantum coherence by a frequency-selective pair of pr2 pulses. The z