<p>The field of nuclear magnetic resonance has experienced a number of spectacular developments during the last decade. Fourier transform methodology revolutionized signal acquisition capabilities. Superconducting magnets enhanced sensitivity and produced considerable improvement in spectral dispers
Multinuclear NMR
โ Scribed by Joan Mason (auth.), Joan Mason (eds.)
- Publisher
- Springer US
- Year
- 1987
- Tongue
- English
- Leaves
- 641
- Edition
- 1
- Category
- Library
No coin nor oath required. For personal study only.
โฆ Synopsis
With the power and range of modern pulse spectrometers the compass of NMR specยญ troscopy is now very large for a single book-but we have undertaken this. Our book covers the Periodic Table as multinuclear spectrometers do, and introductory chapters are devoted to the essentials of the NMR experiment and its products. Primary products are chemical shifts (including anisotropies), spin-spin coupling constants, and relaxation times; the ultimate product is a knowledge of content and constitution, dynamic as well as static. Our province is chemical and biochemical rather than physical or technical; only passing reference is made to metallic solids or unstable species, or to practical NMR spectroscopy. Our aim is depth as well as breadth, to explain the fundamental processes, whether of nuclear magnetic shielding, spin-spin coupling, relaxation, or the multiple pulse sequences that have allowed the development of high-resolution studies of solids, multidimensional NMR spectroscopy, techniques for sensitivity enhancement, and so on. This book therefore combines the functions of advanced textbook and reference book. For reasonably comprehensive coverage in a single volume we have sumยญ marized the information in tables and charts, and included all leading references.
โฆ Table of Contents
Front Matter....Pages i-xx
Introduction....Pages 1-2
The Parameters of NMR Spectroscopy....Pages 3-50
The Chemical Shift....Pages 51-88
Spin-Spin Coupling....Pages 89-131
Relaxation and Related Time-Dependent Processes....Pages 133-169
Hydrogen and Its Isotopes....Pages 171-187
The Alkali and Alkaline Earth Metals....Pages 189-220
Boron....Pages 221-258
Aluminum, Gallium, Indium, and Thallium....Pages 259-292
Carbon....Pages 293-303
Silicon, Germanium, Tin, and Lead....Pages 305-333
Nitrogen....Pages 335-367
Phosphorus to Bismuth....Pages 369-402
Oxygen....Pages 403-416
Sulfur, Selenium, and Tellurium....Pages 417-435
Fluorine....Pages 437-446
The Quadrupolar Halides....Pages 447-461
The Noble Gases....Pages 463-477
Early Transition Metals, Lanthanides and Actinides....Pages 479-519
Group VIII Transition Metals....Pages 521-561
Post-Transition Metals, Copper to Mercury....Pages 563-589
NMR Spectroscopy in Bioinorganic Chemistry....Pages 591-604
Biomedical NMR....Pages 605-614
Back Matter....Pages 615-639
โฆ Subjects
Biochemistry, general; Biotechnology; Analytical Chemistry
๐ SIMILAR VOLUMES
<div><p>This book presents several helpful synthetic methods for diverse multinuclear complexes. The results described can be used to selectively connect mononuclear as well as multinuclear complexes with other metal complexes to construct valuable photofunctional compounds. Using the new synthetic