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Mukaiyama and Torgov Chemistry in the Synthesis of (D-Homo) Steroid Skeletons

✍ Scribed by Florence C. E. Saraber; Svetlana V. Drach; Alexander Baranovsky; Tanya Charnikhova; Serghei Pogrebnoi; Ben J. M. Jansen; Aede de Groot

Book ID
101991388
Publisher
John Wiley and Sons
Year
2006
Weight
8 KB
Volume
37
Category
Article
ISSN
0931-7597

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A short and efficient procedure has been developed for the synthesis of C,D-cis coupled steroid and D-homo steroid skeletons. A Mukaiyama reaction with transfer of the silyl group of the starting silyl enol ether to the enol of the adduct followed by addition of vinyl magnesium bromide to the unprot