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Monomere Tris(η2-pyrazolato)-Lanthanoidkomplexe mit dem sterisch anspruchsvollen 3,5-Di(tert-butyl)pyrazolatoliganden

✍ Scribed by Joanna E. Cosgriff; Dr. Glen B. Deacon; Dr. Bryan M. Gatehouse; Holger Hemling; Prof. Dr. Herbert Schumann

Publisher
John Wiley and Sons
Year
1993
Tongue
English
Weight
285 KB
Volume
105
Category
Article
ISSN
0044-8249

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Monomeric Tris(η2-pyrazolato)Lanthanoid
Monomeric Tris(η2-pyrazolato)Lanthanoid Complexes with the Bulky 3,5-Di(tert-butyl)pyrazolato Ligand
✍ Joanna E. Cosgriff; Dr. Glen B. Deacon; Dr. Bryan M. Gatehouse; Dipl.-Chem. Holg 📂 Article 📅 1993 🏛 John Wiley and Sons 🌐 English ⚖ 291 KB

1,3.5-Tris[diazo(3-(diazo(3-(diazo(phenyl)methyl)phenyl)methyl)phenyl)methyllbenzene (4d): The nonaketone 4 b was converted to the corresponding nonahydrazone 4 c by the addition of anhydrous hydrazine and hydrazine hydrochloride in dimethyl sulfoxide (DMSO) at 90'C. The nonahydrazone 4c was then o