Monolith as a new sample preparation material: Recent devices and applications
✍ Scribed by Akira Namera; Akihiro Nakamoto; Takeshi Saito; Shota Miyazaki
- Publisher
- John Wiley and Sons
- Year
- 2011
- Tongue
- English
- Weight
- 350 KB
- Volume
- 34
- Category
- Article
- ISSN
- 1615-9306
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
Monolith was first used as a material for chromatographic separation two decades ago and solid‐phase extraction over 10 years, and since then, separation science has undergone a dramatic change owing to advancements in analytical technology. Recently, monolith has been modified to suit various devices for the extraction and enrichment of analytes in any matrices of environmental, food, and biological analyses. This approach has contributed to miniaturization and automation for sample preparation, and it can reduce the time and cost requirements of sample preparation. Recently, numerous applications have been demonstrated for online and inline preconcentration coupled with monolith, and many kinds of devices have been designed and developed for offline devices. In this review, these applications and devices are listed and discussed in reference to other fields.
📜 SIMILAR VOLUMES
## Abstract In this study, a new stir bar sorptive extraction (SBSE) coating based on poly(vinylphthalimide‐__co__‐__N__,__N__′‐methylenebisacrylamide) monolith (SBSE‐VPMB) was prepared. The influences of the contents of monomer in polymerization mixture and the percentage of porogen solvent on the
## Abstract The aim of preoperative embolization is to facilitate surgical removal by reducing tumor volume and vascularity, thereby decreasing blood loss during surgery. In a search for a better embolic material, compared to heterogeneous commercial products, we describe here in detail the prepara
A thermo-responsive polymer on which maltose was covalently immobilized as an affinity ligand was newly synthesized for purification of thermolabile proteins from the crude solution by affinity precipitation. Among the thermo-responsive polymers synthesized as carriers for adsorbent, poly(N-acryloyl
## Abstract Disymmetrically substituted oligo(phenyleneethynediyl) (OPE) derivatives were prepared from 2,5‐bis(octyloxy)‐4‐[(triisopropylsilyl)ethynyl]benzaldehyde (5) by an iterative approach using the following reaction sequence: __i__) __Corey–Fuchs__ dibromoolefination, __ii__) treatment with