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Monitoring electrochemical reactions in situ using steady-state free precession 13C NMR spectroscopy

✍ Scribed by Nunes, Luiza M.S.; Moraes, Tiago B.; Barbosa, Lucio L.; Mazo, Luiz H.; Colnago, Luiz A.


Book ID
124140376
Publisher
Elsevier Science
Year
2014
Tongue
English
Weight
421 KB
Volume
850
Category
Article
ISSN
0003-2670

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High resolution 13C-n.m.r. spectroscopy can be performed in the solid state by taking advantage of 1H-13C cross-polarization (CP) and magic angle spinning (MAS). This technique is presently applied to identify in situ carbonaceous residues from zeolite-catalysed reactions. H-ZSM 5 and H-Mordenite c