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Molecular structure of 9α-fluoro-11β-hydroxy-16β-propionyloxy-17-(2-ethyl-2-ethoxy-1,3-dioxan-5-one-6-yl)-pregna-1,4-dien-3-one

✍ Scribed by Giuliano Bandoli; Marino Nicolini

Publisher
Springer
Year
1982
Tongue
English
Weight
395 KB
Volume
12
Category
Article
ISSN
1572-8854

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Preparation of high specific activity tr
Preparation of high specific activity tritium labeled 6α,9,-difluoro-11β,21-dihydroxy-16α,17-[(1-methylethylidene)bis(oxy)]pregna-1,4-diene-3,20-one, fluocinolone acetonide
✍ D. Zhong; Anita H. Lewin 📂 Article 📅 2009 🏛 John Wiley and Sons 🌐 French ⚖ 289 KB

## Abstract Fluocinolone acetonide was tritiated by selective reduction of the 1,2‐double bond of the __O__‐protected analog under tritium, followed by re‐establishment of the 1,2‐double bond and deprotection. Protection of both hydroxyl functionalities was required. The product was obtained with s