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Molecular structure of 5,6-bis(dimethylamino)acenaphthene, 5,6-bis(dimethylamino)acenaphthylene, and their monohydrobromides: a comparison with some naphthalene proton sponges

✍ Scribed by Pozharskii, Alexander F.; Ozeryanskii, Valery A.; Starikova, Zoya A.


Book ID
121266630
Publisher
Royal Society of Chemistry
Year
2002
Tongue
English
Weight
180 KB
Volume
2
Category
Article
ISSN
1472-779X

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Low-temperature (120 K) studies of the structure of the DMAN Á DCI adduct indicate that in symmetrical [NHN] hydrogen bridge of 2.571 (1) A ˚length (2.579(2) A ˚at room temperature) there is a disorder of the H-atom occupying two positions at nitrogen atoms with a distance of 0.94(3) A ˚. The compa