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Molecular and crystal structure ofβ-dimethylaminoethylα,α-diphenyl-α-ethoxyacetate hydrochloride

✍ Scribed by L. Ya. Erman; V. F. Mindrul; I. L. Mikhaleva; V. K. Kurochkin


Publisher
SP MAIK Nauka/Interperiodica
Year
1994
Tongue
English
Weight
223 KB
Volume
34
Category
Article
ISSN
0022-4766

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CH,(18) + 14-CH3; 2.07, s CH,( 4) (CDCI,);not yet crystalli~ed]~). Finally, 8 was converted by catalytic hydrogenation [5%-Pd/C in ethanol/triethylamine; + 11 and cyclisation [HCl in acetic acid] into 3-oxo-17~-acetoxy-14a-methyl-A4-8a,9B,lOa,13a-estrene (12) [m.p. 86-88'; -[ U ] D = + 1' (CHC1,).