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Molecular Addition Compounds of Amines and Iodine. Evidence for the Existence of a 2:1 Triethylamine-Iodine Complex

✍ Scribed by Schmulbach, C. D.; Hart, D. M.

Book ID: 120041289
Publisher: American Chemical Society
Year: 1964
Tongue: English
Weight: 586 KB
Volume: 86
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja01066a010

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The lithium phthalocyaninate(1-) iodine inclusion complex [(Lipc -)•I], prepared by the reaction of anhydrous lithium iodide with molten 1,2-dicyanobenzene, crystallizes tetragonally in the space group P4/mcc with a = 14.057(3) Å, b = 6.397(1) Å, V = 1264.0(4) Å 3 , Z = 2. Lithium is in a crystallog