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Modern Sample Preparation for Chromatography

✍ Scribed by Serban C. Moldoveanu, Victor David

Publisher
Elsevier
Year
2014
Tongue
English
Leaves
446
Edition
1
Category
Library
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✦ Synopsis

Sample preparation is applied to make real world samples amenable for chromatographic analysis, or to improve the results of this type of analysis. A wide variety of procedures are applied for this purpose, and their description is the main goal of the present book. The principles of these procedures are explained, discussing their advantages and disadvantages, and their applicability to different types of samples as well as their fit for different types of chromatographic analysis. This provides a guide for choosing the appropriate sample preparation for a given analysis. The book also contains numerous literature references and examples of sample preparation for different matrices. The material is presented in three parts, one discussing physical methods used in sample preparation such as filtration, distillation, solvent extraction, solid phase extraction, electro-separations.

* presents in a systematic way numerous techniques applied for sample preparation for chromatographic analysis

* provides an up to date source of information regarding the progress made in sample preparation for chromatography

* describes examples for specific type of matrices, providing a guide for choosing the appropriate sample preparation method for a given analysis

✦ Table of Contents

Content:
Front Matter, Page iii
Copyright, Page iv
Preface, Pages xi-xii
Chapter 1 - Preliminaries to Sample Preparation, Pages 3-32, Serban Moldoveanu, Victor David
Chapter 2 - The Role of Sample Preparation, Pages 33-49, Serban Moldoveanu, Victor David
Chapter 3 - Chromatography as a Core Step for an Analytical Procedure, Pages 51-85, Serban Moldoveanu, Victor David
Chapter 4 - Mechanical Processing in Sample Preparation, Pages 89-104, Serban Moldoveanu, Victor David
Chapter 5 - Phase Transfer in Sample Preparation, Pages 105-130, Serban Moldoveanu, Victor David
Chapter 6 - Solvent Extraction, Pages 131-189, Serban Moldoveanu, Victor David
Chapter 7 - Solid-Phase Extraction, Pages 191-286, Serban Moldoveanu, Victor David
Chapter 8 - Other Sample Preparation Techniques Not Involving Chemical Modifications of the Analyte, Pages 287-305, Serban Moldoveanu, Victor David
Chapter 9 - The Role of Derivatization in Chromatography, Pages 307-331, Serban Moldoveanu, Victor David
Chapter 10 - Chemical Reactions Used in Derivatizations, Pages 333-391, Serban Moldoveanu, Victor David
Chapter 11 - Chemical Degradation of Polymers for Chromatographic Analysis, Pages 393-409, Serban Moldoveanu, Victor David
Chapter 12 - Comments on Sample Preparation in Chromatography for Different Types of Materials, Pages 411-446, Serban Moldoveanu, Victor David
Index, Pages 447-453

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