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Mobility of dichloroethyl radicals sorbed in kaolin and silica: a potential model of heterogeneous atmospheric processes

✍ Scribed by Christopher J. Rhodes; Timothy C. Dintinger; Ivan D. Reid; Christopher A. Scott


Publisher
John Wiley and Sons
Year
2000
Tongue
English
Weight
107 KB
Volume
38
Category
Article
ISSN
0749-1581

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✦ Synopsis


An activation energy of 10.6 š 1.4 kJ mol 1 was determined for the reorientational diffusion of 1,1dichloroethyl radicals sorbed in silica gel by transverse-field muon spin rotation (TF-MuSR) spectroscopy, and was confirmed by longitudinal-field muon spin relaxation (LF-MuSRx) measurements, which gave a value of 10.9 š 0.7 kJ mol 1 . Also according to TF-MuSR measurements, the activation energy for this radical sorbed in kaolin powder is 11.0 š 1.3 kJ mol 1 , which was within experimental error of that obtained from an LF-MuSRx study (12.3 š 0.8 kJ mol 1 ). The LF-MuSRx method also revealed the presence of an additional, more mobile, fraction of 1,1-dichloroethyl radicals in both silica and kaolin with activation energies of 2.6 š 0.4 and 2.4 š 0.2 kJ mol 1 , respectively.