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[Mo4(η3-S)4(η-S2CNEt2)2(S2CNEt2)4], eine Verbindung mit cubanähnlichem Mo4S4-Cluster

✍ Scribed by Prof. Dr. Thomas C. W. Mak; Dr. Khalid S. Jasim; Prof. Dr. Chung Chieh

Publisher
John Wiley and Sons
Year
1984
Tongue
English
Weight
247 KB
Volume
96
Category
Article
ISSN
0044-8249

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Synthesis and Crystal Structures of the Novel Tetrameric Nitrido Complexes [{cyclo-ReN}4(S2CNEt2)6(MeOH)2(PPh3)2][BPh4]2 · CH2Cl2 · 2 H2O and [{cyclo-ReN}4(S2CNEt2)4Cl4(PMe2Ph)4] · 2 acetone
✍ D. V. Griffiths; S. J. Parrott; M. Togrou; J. R. Dilworth; Yifan Zheng; S. Ritte 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 German ⚖ 141 KB 👁 2 views

Novel tetrameric rhenium(V) complexes have been prepared from [ReNCl 2 (PPh 3 ) 2 ] and [ReN(PMe 2 Ph) (S 2 CNEt) 2 ], respectively. [ReNCl 2 (PPh 3 ) 2 ] reacts with 1.5 equivalents of KS 2 CNEt 2 in methanol to yield the unusual dark red species [{cyclo-ReN} 4 (S 2 CNEt 2 . The crystal structure