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Mixing apparatus for preparing NMR samples under pressure

โœ Scribed by Wen-Jin Wu; Gediminas Vidugiris; Ed S. Mooberry; William M. Westler; John L. Markley

Book ID
108487817
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
216 KB
Volume
164
Category
Article
ISSN
1090-7807

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โœ Martin Goez ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 44 KB

A very simple closed apparatus and procedure are described which allow in situ drying of NMR samples by using molecular sieves and the freeze-pump-thaw technique. Limitations of the method are discussed. With acetonitrile, a residual water content of 3 ุ‹ 10 ุŠ4 M could be reached.