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Mismatching Cross Polarization in the Rotating Frame

✍ Scribed by S.M. Zhang; E.O. Stejskal; R.E. Fornes; X.L. Wu

Publisher
Elsevier Science
Year
1993
Tongue
English
Weight
180 KB
Volume
104
Category
Article
ISSN
1064-1858

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A proton dynamic nuclear polarization (DNP) NMR signal enhancement (β‘€) close to thermal equilibrium, β‘€ ‫؍‬ 0.89, has been obtained at high field (B 0 ‫؍‬ 5 T, epr ‫؍‬ 139.5 GHz) using 15 mM trityl radical in a 40:60 water/glycerol frozen solution at 11 K. The electron-nuclear polarization transfer i