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Mild and Direct Conversion of Quinoline N-Oxides to 2-Amidoquinolines with Primary Amides.

โœ Scribed by Michel Couturier; Laurence Caron; Stephanie Tumidajski; Kris Jones; Timothy D. White


Publisher
John Wiley and Sons
Year
2006
Weight
24 KB
Volume
37
Category
Article
ISSN
0931-7597

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โœ Anna Hubacz; Slawomir Makowiec ๐Ÿ“‚ Article ๐Ÿ“… 2009 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 142 KB

The reaction of [di(acyloxy)iodo]benzene with secondary phosphine oxides or H-phosphinates in the presence of primary or secondary amines allows one to obtain phosphinic or phosphonic acids amides in the one-pot process. We take advantage of the strong acylating system DAIB/R 2 P(O)H to phosphinylat