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Microwave oven synthesis of esters promoted by imidazole

✍ Scribed by Takuji Hirose; Benjamin G. Kopek; Zhao-Hui Wang; Ritsuko Yusa; Bruce W. Baldwin


Book ID
104253043
Publisher
Elsevier Science
Year
2003
Tongue
French
Weight
156 KB
Volume
44
Category
Article
ISSN
0040-4039

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✦ Synopsis


Using imidazole as promotion agent, primary, secondary and phenolic alcohol compounds were esterified with aliphatic and aromatic carboxylic acid anhydrides. Heating a ternary mixture of alcohol, anhydride and imidazole in an unmodified microwave oven produced esters in low to high yields, depending on the steric bulk of the alcohol.


πŸ“œ SIMILAR VOLUMES


Microwave Oven Synthesis of Esters Promo
✍ Takuji Hirose; Benjamin G. Kopek; Zhao-Hui Wang; Ritsuko Yusa; Bruce W. Baldwin πŸ“‚ Article πŸ“… 2003 πŸ› John Wiley and Sons βš– 91 KB

## Abstract For Abstract see ChemInform Abstract in Full Text.

Application of commercial microwave oven
✍ Raymond J Giguere; Terry L Bray; Scott M Duncan; George Majetich πŸ“‚ Article πŸ“… 1986 πŸ› Elsevier Science 🌐 French βš– 259 KB

## SmauTr Cormereisl microwave ovens have been safely used to dramatically reduce the reaction times (at c-arable yield) of Diels-Alder, Claiscn, and ene reactions. Significant solvent effects were ~180 observed.