✦ LIBER ✦
Microwave-enhanced, solvent-free synthesis of singly and doubly 13C-labelled trans-cinnamic acid at the α- and β-carbon positions
✍ Scribed by Guibin Ma; Sophia E. Hayes
- Publisher
- John Wiley and Sons
- Year
- 2004
- Tongue
- French
- Weight
- 120 KB
- Volume
- 47
- Category
- Article
- ISSN
- 0022-2135
- DOI
- 10.1002/jlcr.878
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✦ Synopsis
Abstract
^13^C‐labelled trans‐cinnamic acid (3‐phenyl‐2‐propenoic acid) has been synthesized in one step using benzaldehyde‐carbonyl‐^13^C and malonic acid‐2‐^13^C in the presence of ammonium acetate under microwave irradiation and solvent‐free conditions. Copyright © 2004 John Wiley & Sons, Ltd.