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Microwave-Assisted Synthesis of Tricarbonyl Rhenacarboranes: Steric and Electronic Effects on the 1,2 → 1,7 Carborane Cage Isomerization

✍ Scribed by Armstrong, Andrea F.; Valliant, John F.

Book ID: 125540508
Publisher: American Chemical Society
Year: 2007
Tongue: English
Weight: 364 KB
Volume: 46
Category: Article
ISSN: 0020-1669
DOI: 10.1021/ic0617543

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## Abstract Four bicyclic dioxetanes bearing a phenolic substituent, 3‐__tert__‐butyldimethylsiloxy‐4‐chlorophenyl (**3a**), 5‐__tert__‐butyldimethylsiloxy‐4‐chloro‐2‐ethylphenyl (**3b**), 5‐__tert__‐butyldimethylsiloxy‐2‐ethylphenyl (**3c**), and 3‐__tert__‐butyldimethylsiloxy‐4‐ethylphenyl (**3d*