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Microwave-assisted synthesis of resorcin[4]arene and pyrogallol[4]arene macrocycles

✍ Scribed by Muriel Funck; Daniel P. Guest; Gareth W.V. Cave

Publisher
Elsevier Science
Year
2010
Tongue
French
Weight
505 KB
Volume
51
Category
Article
ISSN
0040-4039

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✦ Synopsis

A series of resorcin [4]arene and pyrogallol[4]arene macrocycles have been synthesized efficiently within 5 min, affording crystalline products suitable for single crystal X-ray diffraction, utilising microwave irradiation in a 'one-pot' reaction whilst controlling the selective formation of the rccc cone stereoisomer.

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