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Microwave-assisted synthesis of d-glucuronic acid derivatives using cost-effective solid acid catalysts

✍ Scribed by Aurore Richel; Pascal Laurent; Bernard Wathelet; Jean-Paul Wathelet; Michel Paquot

Publisher
Elsevier Science
Year
2010
Tongue
French
Weight
247 KB
Volume
51
Category
Article
ISSN
0040-4039

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✦ Synopsis

Monomode microwave-assisted coupling of D-glucuronic acid with alcohols, in the presence of various impregnated acid catalysts, was successfully performed, affording in almost quantitative yields the corresponding monosubstituted b-D-glucofuranosidurono-6,3-lactones in less than 10 min at 85 Β°C. This study evidences the synergy of microwaves and impregnated acid catalysts as a fast and clean strategy in the field of carbohydrate chemistry.

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