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Microwave-assisted synthesis, metallation, and duff formylation of porphyrins
β Scribed by Muhammad Yaseen; Mukhtar Ali; Muhammad NajeebUllah; Munawar Ali Munawar; Irshad Khokhar
- Book ID
- 102344278
- Publisher
- Journal of Heterocyclic Chemistry
- Year
- 2009
- Tongue
- English
- Weight
- 134 KB
- Volume
- 46
- Category
- Article
- ISSN
- 0022-152X
- DOI
- 10.1002/jhet.78
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β¦ Synopsis
Abstract
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Microwave assisted synthesis, metallation, and Ξ²βformylation of porphyrins is described. All synthetic reactions were carried out on inorganic polymer solid support using microwave energy. It is the first documented application of the Duff reaction in the field of porphyrins and metalloporphyrins. The overall process is simple, easy, and environment friendly. FTIR, UVβvisible, elemental analysis, ^1^H NMR, and mass spectrometry were used to characterize the compounds. J. Heterocyclic Chem., 46, 251 (2009).
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