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Microwave-assisted synthesis, crystal structures and thermal behaviour of Na5Y(CO3)4 and Na5Yb(CO3)4·2H2O

✍ Scribed by M.O. Awaleh; A. Ben Ali; V. Maisonneuve; M. Leblanc


Book ID
117621289
Publisher
Elsevier Science
Year
2003
Tongue
English
Weight
743 KB
Volume
349
Category
Article
ISSN
0925-8388

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Differential scanning calorimetry (DSC) and X-ray diffraction measurements have been performed on pentasodium trihydrogen tetraselenate dihydrate Na 5 H 3 (SeO 4 ) 4 •2H 2 O and deuterated Na 5 D 3 (SeO 4 ) 4 •2D 2 O crystals. Any distinct anomaly around 428 K in the DSC curves for both crystals is