✦ LIBER ✦
Microwave-Assisted Rapid Incorporation of Ruthenium into Lacunary Keggin-Type Polyoxotungstates: One-Step Synthesis, 99Ru, 183W NMR Characterization and Catalytic Activity of [PW11O39RuII(DMSO)]5–
✍ Scribed by Alessandro Bagno; Marcella Bonchio; Andrea Sartorel; Gianfranco Scorrano
- Publisher
- John Wiley and Sons
- Year
- 2000
- Tongue
- English
- Weight
- 233 KB
- Volume
- 2000
- Category
- Article
- ISSN
- 1434-1948
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✦ Synopsis
Microwave irradiation for 15 minutes allowed the highly stable oxidation catalyst [PW 11 O 39 Ru II (DMSO)] 5-, as confirmed by 1 H, 31 P, 99 Ru and 183 W NMR techniques. selective hydrothermal synthesis of the diamagnetic, airgeometries of both 2 and 3 obtained with PM3(tm) semiem- [a