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Microwave-Assisted, One-Pot Synthesis of 5-Thia-4 b ,10-diaza-indeno[2,1- a ]-indene-5,5-dioxide and 10 H -11-Thia-5,10 a -diaza-benzo[ b ]fluorene-11,11-dioxide

✍ Scribed by Cole, Andrew G.; Kultgen, Steven G.; Henderson, Ian


Book ID
126603261
Publisher
Taylor and Francis Group
Year
2009
Tongue
English
Weight
167 KB
Volume
39
Category
Article
ISSN
0039-7911

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## Abstract The title novel fused tricyclic phosphoroheterocycle, C~19~H~20~N~3~O~2~PS, was synthesized in an excellent yield of 88.5% via the reac‐ tion of 1‐(2‐bromoethyl)‐2,3‐dihydro‐3‐propyl‐1,3,2‐benzodiazaphosphorin‐4(1__H__)‐one 2‐oxide with phenyl isothiocyanate, which contains the proximat