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Microwave-Assisted Dimroth Rearrangement of Thiazines to Dihydropyrimidinethiones: Synthetic and Mechanistic Aspects.

✍ Scribed by Toma N. Glasnov; Danielle J. Vugts; Manoe M. Koningstein; Bimbisar Desai; Walter M. F. Fabian; Romano V. A. Orru; C. Oliver Kappe

Publisher
John Wiley and Sons
Year
2006
Weight
22 KB
Volume
37
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

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Synthetic and Theoretical Aspects of New Dimroth Rearrangement of6-Aminopyran-2-ones to 6-Hydroxypyridin-2-ones via Carbamoyl Ketenes
✍ Julia O. Subbotina; Walter M. F. Fabian; Evgeniy V. Tarasov; Natalia N. Volkova; 📂 Article 📅 2005 🏛 John Wiley and Sons 🌐 English ⚖ 176 KB

## Abstract Two alternative directions for thermal transformation of 6‐amino‐4‐oxopyrano[3,4‐__d__] [1,2,3]thiadiazoles **1**, leading either to 6‐hydroxy‐4‐oxo‐[1,2,3]thiadiazolo[4,5‐__c__]pyridines **2** or 2‐cyano‐2‐(1,2,3‐thiadiazol‐5‐yl)acetamide **4b**, were observed. The first one represents