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Microstructure and growth mechanism of PtAl2O3 co-sputtered nanocermet films studied by SAXS, TEM and AFM

✍ Scribed by C. Sella; M. Mâaza; B. Pardo; F. Dunsteter; J.C. Martin; M.C. Sainte Catherine


Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
302 KB
Volume
241
Category
Article
ISSN
0378-4371

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✦ Synopsis


The physical properties of nanocermets are related mostly to their morphology. In this contribution, we present the microstructural and morphological evolution of co-sputtered Pt-AlzO 3 granular films with thickness, metal concentration and thermal annealing. These investigations are achieved by grazing angle X-ray reflectometry, transmission electron microscopy and atomic force microscopy. The experimental results show that (i) the diameter of platinum clusters increases as a function of film thickness, annealing temperature and metal concentration and (ii) a columnar growth is observed whose morphology also depends on the previous parameters and on the growth direction.