𝔖 Bobbio Scriptorium
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Microscopic identification of ephedrine with nitrous acid

✍ Scribed by Grill, Frederick


Publisher
Elsevier
Year
1932
Weight
345 KB
Volume
21
Category
Article
ISSN
0898-140X

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During the irradiation of phenol (1) with 15 N-enriched tetranitromethane in acetonitrile, and during the reaction of 1 with 15 N-enriched nitric acid and nitrous acid, emission due to the nitration products o-and p-nitrophenol (2a, 2b) is observed in the 15 N-NMR spectra. The CIDNP effects are buil