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Microcolumn chromatography for the analysis of detergents and lubricants. Part 1: High temperature capillary gas chromatography (HT-CGC) and capillary supercritical fluid chromatography (CSFC)

✍ Scribed by Sandra, Pat ;David, Frank

Publisher
John Wiley and Sons
Year
1990
Tongue
English
Weight
332 KB
Volume
13
Category
Article
ISSN
0935-6304

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✦ Synopsis

Abstract

High Temperature Capillary GC and Capillary SFC have been applied to the analysis of non‐ionic lubricants, i.e. alkylphenol polyethoxylates (APnEO), ethoxylated alcohols (nEOAIc), polyethylene glycols (PEG), and ethoxylated triethanolamines (nEOEA); to the analysis of anionic lubricants, i.e. alkylbenzene‐sulfonates (ABS), alkylsulfonates (AS), and ethoxylated phosphoric acids (nEOPhA); and to the analysis of cationic lubricants, i.e. quaternary ammonium salts (Quats). Both techniques are compared in terms of resolution and analysis time. The importance of derivatization in HT‐CGC and CSFC is illustrated.

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