✦ LIBER ✦
Micro-bomb combustion calorimeter equipped with an electric heater for aiding complete combustion
✍ Scribed by Minoru Sakiyama; Tetsu Kiyobayashi
- Publisher
- Elsevier Science
- Year
- 2000
- Tongue
- English
- Weight
- 184 KB
- Volume
- 32
- Category
- Article
- ISSN
- 0021-9614
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✦ Synopsis
A micro-bomb oxygen combustion calorimeter suitable for samples with masses of about 20 mg is described. In order to prevent incomplete combustion, a small heater is fitted under the crucible. The calorimeter was tested by determining the standard molar enthalpy of formation of salicylic acid in the crystalline state at T = 298.15 K: f H • m (cr)/ (kJ • mol -1 ) = (588.4 ± 1.7).