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Michael and Mannich reactions with benzothiazole-2-thiol

โœ Scribed by Halasa, Adel F.; Smith, George E. P.

Book ID
120181150
Publisher
American Chemical Society
Year
1971
Tongue
English
Weight
712 KB
Volume
36
Category
Article
ISSN
0022-3263

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Mechanism of formation of benzothiazole-
Mechanism of formation of benzothiazole-2-thiol
โœ Neil S. Isaacs; Fyaz Ismail; Mark J. Hilton; Mark Coulson ๐Ÿ“‚ Article ๐Ÿ“… 1998 ๐Ÿ› John Wiley and Sons ๐ŸŒ English โš– 232 KB ๐Ÿ‘ 2 views

The formation of benzothiazole-2-thiol from aniline, carbon disulphide and sulphur at 230ยฐC was shown to occur by a sequence of three principal steps. Labelling experiments confirmed that both sulphur atoms originate from carbon disulphide. An initial polar reaction to form thiocarbanilide via pheny