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Methyltrioxorhenium-Catalyzed Oxidation of Aromatic Aldoximes.

✍ Scribed by Francesca Cardona; Gianluca Soldaini; Andrea Goti

Publisher
John Wiley and Sons
Year
2004
Weight
24 KB
Volume
35
Category
Article
ISSN
0931-7597

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## Methoxy-substituted benzenes 1 are oxidized with aqueous hydrogen peroxide catalyzed by methyltrioxorhenium( VII) in acetic acid to yield the p-benzoquinones 3 in moderate yields. An intermediary diperoxo rhenium(W) complex rather than peracetic acid is the dominating oxidizing species, since o