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Methyl Group Internal Rotation Dynamics: Overtone Study of Gaseous Methylpyridine-2-α d 2 and -3-α d 2

✍ Scribed by Bergeat, A.; Cavagnat, D.; Lapouge, C.; Lespade, L.

Book ID
126772766
Publisher
American Chemical Society
Year
2000
Tongue
English
Weight
183 KB
Volume
104
Category
Article
ISSN
1089-5639

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## Abstract Methyl 2‐__O__‐benzyl‐6‐deoxy‐3‐__C__‐methyl‐α‐D‐mannopyranoside (2) was synthesized in ten steps by starting from the readily available methyl 2,3‐anhydro‐4,6‐__O__‐benzylidene‐α‐D‐allo‐pyranoside (3). The key step was the stereoselective __cis__‐hydroxylation (cat. osmium(VIII) oxide)