𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Methyl 11,2,3,3a-5a-hydr­oxy-1-methyl-10-oxo-4-phenyl 10H-indeno[1,2-b]furo[3,4-b]pyrrole-3a-carboxyl­ate

✍ Scribed by Selvanayagam, S. ;Joy, Anju ;Velmurugan, D. ;Ravikumar, K. ;Raghunathan, R.


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
268 KB
Volume
61
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


In the title compound, C 22 H 21 NO 5 , the pyrrolidine ring and the five-membered ring in the indene group have envelope conformations, while the furan ring adopts a twist conformation. Weak intermolecular C-HÁ Á ÁO interactions link the molecules into centrosymmetric dimers. The crystal packing is further stabilized by van der Waals forces.


📜 SIMILAR VOLUMES


Methyl 5-methyl-3,4-di­phenyl-1H-pyrrole
✍ Light, Mark E. ;Camiolo, Salvatore ;Gale, Philip A. ;Hursthouse, Michael B. 📂 Article 📅 2001 🏛 International Union of Crystallography 🌐 English ⚖ 188 KB

Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.005 A Ê R factor = 0.060 wR factor = 0.171 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Methyl 2-methyl-5-oxo-4-(2-thienyl)-1,5,
✍ Vrábel, Viktor ;Kožíšek, Jozef ;Marchalín, Štefan ;Svoboda, Ingrid 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 196 KB

Methyl 2-methyl-5-oxo-4-(2-thienyl)-1,5,7,8,9,10hexahydro-4H-pyrido[2 0 0 0 ,3 0 0 0 :3 Viktor Vra ´bel, a \* Jozef Koz ˇı ´s ˇek, b S ˘tefan Marchalı ´nc and

(1aS,1bS,4aR,4bR,7aS,10R)-Methyl 1a,1b,4
✍ Hörger, Rolf ;Marsch, Michael ;Geyer, Armin ;Harms, Klaus 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 179 KB

The absolute configuration of the title tetracyclic bis-oxazine, C 14 H 17 N 3 O 5 S, has been determined. It is an unexpected product from the attempt to synthesize a new class of bisoxazolines. The seven-membered lactam ring exhibits four axial (O and N) and one equatorial (S) substituents. The or

(3aS,5aR,10aS,11aR)-2,2-Di­methyl-3a,9,1
✍ Vrábel, Viktor ;Kožíšek, Jozef ;Langer, Vratislav ;Marchalín, Štefan ;Bobošíková 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 242 KB

Single-crystal X-ray study T = 183 K Mean '(C±C) = 0.003 A Ê R factor = 0.035 wR factor = 0.082 Data-to-parameter ratio = 12.6 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.