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Method of Storage of Solid Steel Samples for Hydrogen Analysis

✍ Scribed by Yao, Y. L.; Milliken, K. S.


Book ID
126223566
Publisher
American Chemical Society
Year
1953
Tongue
English
Weight
147 KB
Volume
25
Category
Article
ISSN
0003-2700

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A method is described for the determination of hydrogen in solid samples. The sample is heated under vacuum after which the evolved gases are separated by gas chromatography with a helium ionization detector. The system is calibrated by injecting known amounts of hydrogen, as determined manometrical