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Metastability and microstructure evolution in the synthesis of inorganics from precursors

✍ Scribed by C.G Levi


Publisher
Elsevier Science
Year
1998
Tongue
English
Weight
846 KB
Volume
46
Category
Article
ISSN
1359-6454

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Scheme 2. Reagents and conditions: (a) p-TsCl, pyridine, dry CH 2 Cl 2 , 0Β°C-rt, 14 h; (b) LiAlH 4 , dry THF, 0Β°C-rt, 18 h; (c) NaH, PMBBr, dry THF, 0Β°C-rt, 4 h; (d) 60% aq. AcOH, cat. HCl, rt, 14 h; (e) NaIO 4 , MeOH/H 2 O (2:1), rt, 2 h; (f) Ph 3 P CHCOO(CH 2 ) 2 SO 2 Tol, 110Β°C, 1 h; (g) cat. HCl