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Metal-Mediated Variants of the Passerini Reaction: A New Synthesis of 4-Cyanooxazoles.

✍ Scribed by Qian Xia; Bruce Ganem

Publisher: John Wiley and Sons
Year: 2003
Weight: 143 KB
Volume: 34
Category: Article
ISSN: 0931-7597
DOI: 10.1002/chin.200306131

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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m. p.=248-250GC (dec.; from methanol); [.ID= -129.' (DMSO, c = 1.00); 'H-NMR (D6-DMSO); t=4.13 and 4.18 (s, I-H+l'-H and s, 2 2-benzyl-H, or vice versa); MS: 520 (M+)]. The amino ketone ( 8 ) is probably first formed, being later aromatized by dimerization and air oxidation to yield ( 9 ) . The firs