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Metabolic study of 2-(acetyl-imino)-3-[2-hydroxy-2-(2-thienyl)-ethyl]-thiazoline in chickens. Detection of an active metabolite, 5,6-dihydro-6-(2-thienyl)-imidazo[2,1-b]thiazole

✍ Scribed by Fernand T. N. Allewijn; Paul J. A. Demoen


Publisher
John Wiley and Sons
Year
1966
Tongue
English
Weight
404 KB
Volume
55
Category
Article
ISSN
0022-3549

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✦ Synopsis


After oral treatment of chickens with antazonite (R 6438), six basic products have been found by thin-layer chromatography in extracts of feces, one of them being the parent compound. The most important metabolite (metabolite No. 3) was isolated by column chromatography, and its structure was elucidated by physicochemical methods and confirmed by synthesis and analysis. The new product, 5,6-dihydro-6-(2-thienyl)-imidazo[2,1-b]thiazole (antienite, R 8 141) was about 4 times as active as the original compound. There is some evidence suggesting that the anthelmintic activity of R 6438 is due to this metabolite. Two other metabolites were identified by comparison with existing substances o n thin-layer chromatoplates. Further synthetic and parasitological work has shown that chemical modification of R 8141 may result in still more active substances. The most interesting analog, 2,3,5,6tetrahydro-6-phenyl-imidazo[2,1-b] thiazole (tetramisole, R 8299) has been chosen for further detailed parasitological and pharmacological investigation.