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Medium-vacuum centrifugal molecular distillation in the isolation of high-boiling and heat-sensitive compounds. Part III Epoxy monomer/polymer mixtures

✍ Scribed by GJ Rees

Publisher
Elsevier Science
Year
1976
Tongue
English
Weight
367 KB
Volume
26
Category
Article
ISSN
0042-207X

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✦ Synopsis

Laboratory centrifugal molecular distillation is described for the processing of an epoxy monomer/polymer mixture. Optimum operating conditions are outlined for separation of pure monomer from polymer at low temperature and feed-rate. Viscosity, epoxy values and n.m.r. spectra are utilised to characterise the distillate fractions to establish purity of products. The work concludes the series of papers describing the chemical process applications of medium-vacuum techniques.

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