Mechanism of Si3N4nucleation during carbothermal reduction of silica
β Scribed by M. V. Vlasova; T. S. Bartnitskaya; L. L. Sukhikh; L. A. Krushinskaya; T. V. Tomila; S. Yu. Artyuch
- Publisher
- Springer
- Year
- 1995
- Tongue
- English
- Weight
- 899 KB
- Volume
- 30
- Category
- Article
- ISSN
- 0022-2461
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Sample controlled reaction temperature (SCRT) has been used for the first time to study the kinetics of the carbothermal reduction of silica in nitrogen to obtain silicon nitride (Si 3 N 4 ). It is noteworthy to point out that SCRT method allows both a good control of pressure in the sample surroun
opens a new and convenient way to apply metallofullerenes in nanotechnologies. ## Experimental Sc@C 82 was synthesized by the KrΓ€tschmerΒ±Huffman method, and isolated by multiple-step high-performance liquid chromatography (Japan Analytical Industry Co., Ltd) using Buckyprep and Buckyclutcher colu