Measurements of heteronuclear dipolar powder patterns due only to directly bonded couplings

✍ Scribed by Toshihito Nakai; Takehiko Terao

• Book ID: 102523853
• Publisher: John Wiley and Sons
• Year: 1992
• Tongue: English
• Weight: 261 KB
• Volume: 30
• Category: Article
• ISSN: 0749-1581
• DOI: 10.1002/mrc.1260300109

✦ Synopsis

Abstract

A method is proposed which allows a simple Pake doublet due only to the directly bonded CH pair to be obtained by measuring the local field at the position adjacent to a ^13^C nucleus under proton homonuclear decoupling. This approach allows precise determination of the CH distance even in compounds with high proton density.