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Measurement of two- and three-bond13C−1H J couplings to the Cδcarbons of leucine residues in staphylococcal nuclease

✍ Scribed by Geerten W. Vuister; Toshimasa Yamazaki; Dennis A. Torchia; Ad Bax


Publisher
Springer Netherlands
Year
1993
Tongue
English
Weight
660 KB
Volume
3
Category
Article
ISSN
0925-2738

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Measurement of Small One-Bond Proton–Car
✍ Tran Nghia Pham; Tibor Liptaj; Krystyna Bromek; Dušan Uhrı́n 📂 Article 📅 2002 🏛 Elsevier Science 🌐 English ⚖ 289 KB

Two 2D J-modulated HSQC-based experiments were designed for precise determination of small residual dipolar one-bond carbon-proton coupling constants in (13)C natural abundance carbohydrates. Crucial to the precision of a few hundredths of Hz achieved by these methods was the use of long modulation