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Measurement of Orientation Distributions Using Chemical Shift Amplification

✍ Scribed by Charles Crockford; Helen Geen; Jeremy J. Titman

Publisher
Elsevier Science
Year
2002
Tongue
English
Weight
771 KB
Volume
22
Category
Article
ISSN
0926-2040

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✦ Synopsis

A new three-dimensional magic angle spinning (MAS) experiment is proposed, based on a combination of the two-dimensional rotor-synchronized MAS experiment of Spiess and co-workers and a new chemical shift anisotropy amplification method. The new experiment is demonstrated on a macroscopically ordered sample of ultra-high molecular weight poly(ethylene).

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