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Measurement of long-range 13C-13C J couplings in a 20-kDa protein-peptide complex

✍ Scribed by Bax, Ad; Max, David; Zax, David


Book ID
126162242
Publisher
American Chemical Society
Year
1992
Tongue
English
Weight
397 KB
Volume
114
Category
Article
ISSN
0002-7863

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Long-range J(15N,13C) and J(13C,13C) cou
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Chiral synthons containing either 13Cor 15N-labelled glycine were prepared. The 13C and 15N NMR spectra of the Ni(II) complex of the Schi † base of (S)-2-(N-benzylprolyl)aminobenzophenone and 13C-1-, 13C-2or 15N-labelled glycine were measured and assigned. The observed splitting of the carbon signal