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Measurement of fast proton exchange rates in isotopically labeled compounds

✍ Scribed by Gemmecker, Gerd; Jahnke, Wolfgang; Kessler, Horst

Book ID
118005031
Publisher
American Chemical Society
Year
1993
Tongue
English
Weight
300 KB
Volume
115
Category
Article
ISSN
0002-7863

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We have used a modified version of a previously proposed technique, MEXICO [Gemmecker et al. (1993) J. Am. Chem. Soc., 115, 11620], and improved data analysis procedures in order to measure rapid hydrogen exchange (HX) rates of amide protons in peptides labeled only with 15N. The requirement of 13C-