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Measurement of eight scalar and dipolar couplings for methine–methylene pairs in proteins and nucleic acids

✍ Scribed by Emeric Miclet; Jérôme Boisbouvier; Ad Bax


Publisher
Springer Netherlands
Year
2005
Tongue
English
Weight
685 KB
Volume
31
Category
Article
ISSN
0925-2738

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Measurement of Dipolar Couplings for Met
✍ Marcel Ottiger; Frank Delaglio; John L. Marquardt; Nico Tjandra; Ad Bax 📂 Article 📅 1998 🏛 Elsevier Science 🌐 English ⚖ 153 KB

A simple and effective method is described for simultaneously measuring dipolar couplings for methine, methylene, and methyl groups in weakly oriented macromolecules. The method is a Jmodulated 3D version of the well-known [ 1 H-13 C] CT-HSQC experiment, from which the J and dipolar information are